PublicationsRecent publications:85. "High-Lamellar ordering and Amorphous-Like pi-network in Short-Chain Thiazolothiazole-Thiophene Copolymers Lead to High Mobilities" Osaka, I.; Zhang, R.; Suave, G.; Smilgies, D-M.; Kowalewski, T.; McCullough, R. D. Journal of the American Chemical Society 2009, 131(7), 2521-2529. 84. "Regioregular poly(3-hexylthiophene) in a novel conducting amphiphilic block copolymer" Craley, C. R.; Zhang, R.; Kowalewski, T.; McCullough, R. D.; Stefan, M. C. Macromolecular rapid Communications 2009, 30(1) 11-16. 83. "Grignard Metathesis Method (GRIM): Toward a Universal Method for the Synthesis of Conjugated Polymers," Stefan, M. C.; Javier, A. E.; Osaka, I.; McCullough, R. D. Marcomolecules 2008, 42(1), 30-32. 82. "Advances in Molecular Design and Synthesis of Regioregular Polythiophenes," Osaka, I.; McCullough, R. D. Accounts of Chemical Research 2008, 41, 1202-1214. 81. "Highly Disordered Polymer Field Effect Transistors: N-alkyl dithieno[3,2-b:2',3'-d]pyrrole Based Copolymers with Surprisingly High Charge Carrier Mobilities," Liu, J.; Zhang, R.; Sauve,G.; Kowalewski, T.; McCullough, R. J. Am. Chem. Soc. 2008, 130, 13167-13176. 80. "Dispersion of Pristine Carbon Nanotubes Using Conjugated Block Copolymers," Ianhua, J.; Zou, J.; Liu, L.; Chen, H.; 1, Khondaker, S. I.; McCullough, R. D.; Huo, Q.; Zhai, L. Adv. Mater. 2008, 20, 2055-2060. 79."Regioregular Polythiophenes," invited chapter for Thiophene-Based Materials for Electronics and Photonics, Ewbank, P.; Iovu, M.; McCullough, R. D. Wiley, 200. 78. "Regioregular Polythiophene Solar Cells: Material Properties and Performance," Ewbank, P.; Laird, D.; McCullough, R. D. invited book chapter for Organic Photovoltaics: Materials, Device Physics & Manufacturing Technologies, Lavoisier, 2008. 77. "Novel Thiophene-Thiazolothiazole Copolymers for Organic Field-Effect Transistors," Osaka, I.; Sauvé, G.; Zhang, R.; Kowalewski, T.; McCullough, R. D. Adv. Mater. 2007, 19, 4160-4165. 76. "High Field-Effect Mobilities for Diblock Copolymers of Poly(3-hexylthiophene) and Poly(methyl acrylate)," Sauve, G.; McCullough, R. D. Adv. Mater. 2007, 19, 1822-1855 75. "Conducting Regioregular Polythiophene Block Copolymer Nanofibrils Synthesized by Reversible Addition Fragmentation Chain Transfer Polymerization (RAFT) and Nitroxide Mediated Polymerization (NMP)," Macromolecules 2007, 40, 4733-4735. 74. "Conducting block copolymers of regioregular poly(3-hexylthiophene) and poly(methacrylates): Electronic materials with variable conductivities and degrees of 73. "Regioregular Polythiophenes," Jeffries-EL, M.; McCullough, R. D. Handbook of Conducting Polymers, 3rd Edition, 2007, Chapter 9, pgs. 1-49. 72. "Volatile Organic Compound Detection Using Nanostructured Copolymers," Li, B.; Sauve, G.; Iovu, M. C.; Jeffries-EL, M.; Zhang, R.; Cooper, J.; Santhanam, S.; Schultz, L.; Revelli, J. C.; Kusne, A. G.; (Kowalewski, T.; Snyder, J. L.; Weiss, L. E.; Fedder, G. K.;McCullough, R. D.; Lambeth, D. N. Nanoletters 2006, 6, 1598-1602 71. "Conducting Block Copolymer Nanowires Containing Regioregular Poly(3-hexylthiophene) and Polystyrene," J. Macromolecular Science Part A: Pure and Applied Chemistry 2006, 43,1991-2000 (special issue dedicated to Professor Sukant Tripathy). 70. "Nanostructure Dependence of Field-Effect Mobility in Regioregular Poly(3-hexylthiophene) Thin Film Field Effect Transistors," Zhang, R.; Li, B.; Jeffries-EL, M.; Iovu, M.C.; Sauvé, G.; Cooper, J.; Jia, S.; Tristram-Nagle, S.; Smilgies, D. M.; Lambeth, D. N.;McCullough, R. D.; Kowalewski, T. J. Am. Chem. Soc. 2005, 128, 3480-3481. 69. "Facile Synthesis of End-Functionalized Regioregular Poly(3-alkylthiophene)s via Modified Grignard Metathesis Reaction" Malika Jeffries-El, Geneviève Sauvé, and Richard D. McCullough, Macromolecule, 2005, 38, 25, 10346 - 10352. PDF 68. "Experimental Evidence for the Quasi-"Living" Nature of the Grignard Metathesis Method for the Synthesis of Regioregular Poly(3-alkylthiophenes)" Iovu, M. C.; Sheina, E. E.; Gil, R. R.; McCullough, R. D., Macromolecule, 2005, 38, 21, 8649-8656. PDF 67. "Regioregular poly(3-alkylthiophene) Conducting Block Copolymers" Iovu, Mihaela C.; Jeffries-EL, Malika; Sheina, Elena E.; Cooper, Jessica R.; McCullough, Richard D. Polymer, 2005, 46, 19, 8582-8586. PDF 68. "Highly Conductive, Regioregular Alkoxy-Functionalized Polythiophenes: A New Class of Stable, Low Band Gap Materials" Sheina, Elena E.; Khersonsky, Sonya M.; Jones, Edward G.; McCullough, Richard D. Chemistry of Materials, 2005, 17, 13, 3317-3319. PDF 67. Regioregular Poly(thiophene-3-alkanoic acid)s: Water Soluble Conducting Polymers Suitable for Chromatic Chemosensing in Solution and Solid State, Ewbank, P. C.; Loewe, R. S.; Zhai, L.; Reddinger, J.; Sauvé, G.; McCullough, R. D., Tetrahedron, 2004, 60, pg. 11269-11275. (invited) PDF 66. "Chain Growth Mechanism for Regioregular Nickel-Initiated Cross-Coupling Polymerizations," Sheina, E. E.; Liu, J.; Iovu, M. C.; Laird, D. W.; McCullough, R. D. Macromolecules, 2004, 37, pg. 3526-3528. PDF 65. "In-situ End Group Functionalization of Regioregular Poly(3-alkylthiophene) using the Grignard Metathesis Polymerization Method," Jeffries-EL, M.; Sauvé, G., and McCullough, R. D. Adv. Mater., 2004, 16, No. 12., 1017-1019. PDF 64. "Regioregular Polythiophene/Gold Nanoparticle Hybrid Materials", Zhai, Lei; McCullough, Richard D., J. Mater. Chem. 2004, 14, 141-143. PDF 63. "New Phosphonic Acid Functionalized Regioregular Polythiophenes", Stokes, Kristoffer K.; Heuze, Karine; McCullough, Richard D., Macromolecules 2003, 36, 7114-7118. PDF 62. "Soft-Lithography Patterning of Functionalized Regioregular Polythiophenes", Zhai, Lei; Laird, Darin W.; McCullough, Richard D., Langmuir 2003, 19, 6492-6497. PDF 61. "Complex Nanostructured Materials from Segmented Copolymers Prepared by ATRP", Kowalewski, T.; McCullough Richard D.; Matyjaszewski, K., Eur. Phys. J. E. 2003, 10, 5-16. 60. "A Simple Method to Generate Side-Chain Derivatives of Regioregular Polythiophene via the GRIM Metathesis and Post-polymerization Functionalization", Zhai, Lei; Pilston, Richard L.; Zaiger, Karen L.; Stokes, Kristoffer K.; McCullough, Richard, D.; Macromolecules 2003, 36, 61-64. PDF 59. "End Group Modification of Regioregular Polythiophene through Postpolymerization Functionalization", Liu, Jinsong; McCullough, Richard D.; Macromolecules 2002, 35, 9882-9889. PDF 58. "Layer-by-layer Assembly of Polythiophene", Zhai, Lei; McCullough, Richard D.; Adv. Mater. 2002, 14, 901-905. PDF 57. "Tuning the Electrical Conductivity and Self-assembly of Regioregular Polythiophene by Block Copolymerization: Nanowire Morphologies in New Di- and Triblock Copolymers", Liu, Jinsong; Sheina, Elena; Kowalewski, Tomasz; McCullough, Richard D.; Angewandte Chemie, International Edition 2002, 41, 329-332. PDF 56. "Temperature and Voltage Dependent Optical Properties of Conducting Polymer in Synthetic Opal as Photonic Crystal", Satoh, S.; Kajii, H.; Kawagishi, Y.; Tamura, T.; Fujii, A.; Ozaki, M.; McCullough, R. D.; Yoshino, K., Synth. Met. 2001, 121, 1503-1504. 55. "Regioregular, Head-to-Tail Coupled Poly(3-alkylthiophenes) Made Easy by the GRIM Method: Investigation of the Reaction and the Origin of Regioselectivity", Loewe, Robert S.; Ewbank, Paul C.; Liu, Jinsong; Zhai, Lei; McCullough, Richard D., Macromolecules 2001, 34, 4324-4333. PDF 54. "Amine Functionalized Polythiophenes: Synthesis and Formation of Chiral, Ordered Structures on DNA Substrates", Ewbank, P. C.; Nuding, G.; Suenaga, H.; McCullough, R. D.; Shinkai, S., Tetrahedron Lett. 2001, 42, 155-157. 53. "Effects of Structural Regularity on the Properties of Poly(3-alkylthienylenevinylenes)", Loewe, Robert S.; McCullough, Richard D., Chem. Mater. 2000, 12, 3214-3221. 52. "Toward Highly Fluorescent Polythiophenes: Head-to-tail Coupled Copolymers of 3-(methoxyethoxyethoxymethyl)thiophene and 3-(perfluoroalkyl)thiophene", Pilston, R. L.; McCullough, R. D.; Synth. Met. 2000, 111-112, 433-436. 51. "Self-Assembly of Conjugated Polymers at the Air/Water Interface. Structure and Properties of Langmuir and Langmuir-Blodgett Films of Amphiphilic Regioregular Polythiophenes", Reitzel, Niels; Greve, Daniel R.; Kjaer, Kristian; Howes, Paul B.; Jayaraman, Manikandan; Savoy, Steve; McCullough, Richard D.; McDevitt, John T.; Bjornholm, Thomas, J. Am. chem. Soc. 2000, 122, 5788-5800. PDF Recent publications in non-refereed journals:45. McCullough, R. D.; Sauvé, G.; Li, B.; Jeffries-EL, M.; Santhanam, S.; Schultz, L.; Zhang, R.; Iovu, M. C.; Cooper, J.; Sreedharan, P.; Revelli, J. C.; Kusner, A. G.; Kowalewski, T.; Snyder, J. L.; Weiss, L. E.; Lambeth, D. N.; Fedder, G. K. "Regioregular Polythiophene Nanowires and Sensors", Proceedings of SPIE-The International Society for Optical Engineering, 2005, 5940(Organic Field-Effect Transistors IV), 594005/1-594005/7. PDF 44. Sheina, Eleana E.; Iovu, Mihaela C.; McCullough, Richard D. "Synthesis of Regiospecific Poly(3-substituted-thiophenes) using Ni-diimine-initiated Cross-coupling Polymerization", Polymer Preprints, 2005, 46(2), 1070-1071. PDF 43. Cooper, J.; Zhang, R.; Iovu, M.; McCullough, R.; Kowalewski, T. "Comparative Study of Poly(3-alklthiophene) Triblock Copolymers", Polymer Preprints, 2005, 46(2) PDF 42. Sauve, Genevieve; Iovu, Mihaela C.; Jeffries-EL, Malika; McCullough, Richard D. "Well-defined Poly(3-hexylthiophene)-b-Poly(acrylate) Diblock Copolymers" Polymer Preprints, 2005, 46(2), 496. PDF 41. Iovu, Mihaela C.; Sheina, Elena E.; Javier, Anna; Craley, Casey; Jeffries-EL, Milika; McCullough, Richard D. "Living Radical Polymerization Techniques Applied to the Synthesis of Well-defined Copolymers Containing Regioregular Poly(3-alkylthiophene)", Polymer Preprints, 2005, 46(2), 282-283. PDF 40. Cooper, J. Sreedharan, P. Iovu, M. McCullough, R. "Synthesis and characterization of tri-block copolymers containing regioregular poly(3-alkylthiophene)", Polymer Preprints, 2005, 46(1) PDF 39. Sheina, Elena E.; Iovu, Mihaela C.; McCullough, Richard D. "Mechanism and Kinetics of the Nickel-assisted Cross-coupling Polymerizations of Regioregular 3-Alkyl-functionalized Polythiophenes", Polymer Preprints 2005, 46(1), 682-683. PDF 38. Iovu, Mihaela C.; Sheina, Elena E.; McCullough, Richard D. "Grignard Metathesis (GRIM) Method for the Synthesis of Regioregular Poly(3-alkylthiophenes) with Well-defined Molecular Weights", Polymer Preprints 2005, 46(1), 660-661. PDF 37. Sheina, Elena E.; McCullough, Richard D. "Electrical Properties of Highly Conductive EDOT Based Copolymers", Polymer Preprints 2004, 45(2), 800-801. PDF 36. Iovu, Mihaela C.; Jeffries-EL, Malika; Sheina, Elena E.; Krankowski, Ashley B,; Sauve, Genevieve; McCullough, Richard D. "Synthesis and Characterization of Poly(3-hexylthiophene)-b-Polystyrene Di-block Copolymers", Polymer Preprints 2004, 45(2), 645-646. PDF 35. Jeffries-EL, Malika; Iovu, Mihaela C.; Sheina, Elena; Sauve, Genevieve; McCullough, Richard D. "End Functionalized Poly(3-alkylthiophenes) as Building Blocks for the Synthesis of Diblock Copolymers", Polymer Preprints 2004, 45(2), 551-552. PDF 34. Iovu, Mihaela C.; Sheina, Elena E.; Sauve, Genevieve; Jeffries-El, Malika; Cooper, Jessica; McCullough, Richard D., Synthesis of poly(3-hexylthiophene) di-block copolymers using atom transfer radical polymerization, Polymer Preprints 2004 , 45(1), 278-279. PDF 22. McCullough, Richard D.; Liu, Jingsong; Shiena, Elena; Heuze, Karine; Stokes, Kristoffer; Jayaraman, Manikandan; Bjornholm, Thomas; McDevitt, John T, Self-assembly of amphiphilic conducting polymers into nanowires, nanocircuits, and multifunctional materials, Polymeric Materials Science and Engineering 2001, 84, 858. 18. Zhai, Lei; McCullough, Richard D.; Polymer Preprints, 2001, 42(2), 187. PDF 17. Laird, Darin W; Loewe, Robert S.; Ewbank, Paul C.; Liu, Jinsong; Zhai, Lei; McCullough, Richard, D.; Polymer Preprints, 2001, 42(2), 556. PDF Selected publications prior to year 2000:"A Very Simple Method to Prepare Head-to-Tail Coupled, Regioregular Poly(3-alkylthiophenes) Using Grignard Metathesis," Loewe, R. S.; Khersonsky, S. M.; McCullough, R. D. Adv. Mater. 1999 ,11 , 250-253. PDF "The Chemistry of Conducting Polythiophenes," McCullough, R. D., Adv. Mater. 1998 ,10 , 1-24 (review). INVITED PDF "Regioregular, Head-to-Tail Coupled Poly(3-alkylthiophene) and its Derivatives," McCullough, R. D.; Ewbank, P. C. in the Handbook of Conducting Polymers , 2nd edition, Marcell Dekker, 1998 , Chapter 9. 225-258. INVITED "Optimizing the Synthesis of Tetratellurafulvalene (TTeF)," Herr, D. E.; Mays, M. D.; McCullough, R. D.; Bailey, A. B.; Cowan, D. O., J. Org. Chem. 1996 ,61 , 7006-7011. "Toward Tuning Electrical and Optical Properties in Conjugated Polymers Using Side-Chains: The Synthesis and Physical Properties of a Series of the First Head-to-Tail Heteratom Functionalized Polythiophenes," McCullough, R. D.; Williams, S. P., J. Am. Chem. Soc. 1993 ,115 , 11608-11609. PDF "Selective Generation, Isolation, and Purification of Tetrathiafulvalene Tetrathiolate: A Versatile Building Block for New Materials," McCullough, R. D.; Belot, J. A.; Seth, J., J. Org. Chem. 1993 ,58 , 6480-6482. PDF "Self-Oriented Poly(3-Alkylthiophenes): New Insights on Structure-Property Relationships in Conducting Polymers," McCullough, R. D.; Tristram-Nagle, S.; Williams, S. P.; Lowe, R. D.; Jayaraman, M., J. Am. Chem. Soc. 1993 ,115 , 4910-4911. PDF "Design, Synthesis, and Control of Conducting Polymer Architectures: Structurally Homogeneous Poly(3-alkylthiophenes)," McCullough, R.D.; Lowe, R. D.; Jayaraman, M.; Anderson, D. L., J. Org. Chem. 1993 ,58 , 904-912. PDF List of Publications prior to year 2000.
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